TA Instruments

AR1703-0001f

04/09/2012 16:03:28

Sample name	ASW 10 mm from base, 60 mm to top, disk 17 PMMA+FA fouled
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1703
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 16:03:28

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-16.93	7.490	-2.261	1.0040	22.4	749.8	5.3452	10000	0.1840	13.36	6.6815	668.15	3.384E-3	0.0	1.0	61.004	-51.955	5.992
0.9183	12.25	0.07494	2.0040	22.4	749.8	13.1503	10000	0.1840	4.994	16.438	1643.8	3.384E-3	0.0	1.0	62.004	2.8172	9.803
1.600	19.34	0.08276	3.0040	22.4	753.1	26.8498	10000	0.1848	2.014	33.562	3356.2	3.384E-3	0.1	1.1	63.004	4.9102	15.47
2.194	23.02	0.09528	4.0040	22.4	744.0	40.8096	10000	0.1826	1.404	51.012	5101.2	3.384E-3	0.1	1.1	64.004	6.7299	18.42
3.424	30.84	0.1110	5.0040	22.4	757.2	67.5166	10000	0.1858	0.7962	84.396	8439.6	3.384E-3	0.1	1.1	65.004	10.503	24.67
5.539	39.48	0.1403	6.0040	22.4	751.4	106.6360	10000	0.1844	0.4821	133.30	13330	3.384E-3	0.1	1.1	66.004	16.995	31.58
6.244	42.53	0.1468	7.0040	22.4	755.6	126.3060	10000	0.1854	0.4177	157.88	15788	3.383E-3	0.1	1.1	67.004	19.158	34.03
8.163	49.13	0.1661	8.0040	22.4	750.6	165.5030	10000	0.1842	0.3110	206.88	20688	3.384E-3	0.1	1.1	68.004	25.043	39.30
10.71	57.54	0.1862	9.0040	22.4	744.0	223.1520	10000	0.1826	0.2247	278.94	27894	3.384E-3	0.2	1.2	69.004	32.871	46.03
12.70	63.69	0.1994	10.004	22.4	736.5	274.7160	10000	0.1808	0.1816	343.40	34340	3.384E-3	0.2	1.2	70.004	38.970	50.95
14.62	69.65	0.2099	11.004	22.4	744.8	326.0550	10000	0.1828	0.1535	407.57	40757	3.384E-3	0.2	1.2	71.004	44.857	55.72
16.62	75.12	0.2212	12.004	22.4	737.4	378.0020	10000	0.1810	0.1307	472.50	47250	3.383E-3	0.2	1.2	72.004	50.985	60.10
18.65	80.51	0.2316	13.004	22.4	732.4	435.2420	10000	0.1798	0.1130	544.05	54405	3.383E-3	0.2	1.2	73.004	57.210	64.41
20.84	86.43	0.2412	14.000	22.4	718.4	499.1410	10000	0.1763	0.09615	623.93	62393	3.383E-3	0.2	1.2	74.000	63.951	69.15
24.27	94.60	0.2566	15.004	22.4	745.6	594.4830	10000	0.1830	0.08332	743.10	74310	3.384E-3	0.3	1.3	75.004	74.462	75.68
26.33	99.91	0.2635	16.004	22.4	724.1	664.2320	10000	0.1777	0.07254	830.29	83029	3.384E-3	0.3	1.3	76.004	80.779	79.93
29.08	105.7	0.2752	17.004	22.4	730.8	740.6250	10000	0.1794	0.06546	925.78	92578	3.383E-3	0.3	1.3	77.004	89.215	84.53
32.42	113.7	0.2850	18.004	22.4	723.3	855.0400	10000	0.1775	0.05592	1068.8	1.0688E5	3.384E-3	0.3	1.3	78.004	99.453	90.98
34.73	118.8	0.2923	19.004	22.4	711.7	931.2330	10000	0.1747	0.05044	1164.0	1.1640E5	3.384E-3	0.3	1.3	79.004	106.54	95.04
37.71	124.3	0.3035	20.020	22.4	714.2	1020.4900	10000	0.1753	0.04626	1275.6	1.2756E5	3.384E-3	0.3	1.3	80.020	115.68	99.40
41.87	132.3	0.3165	21.008	22.4	696.9	1153.8000	10000	0.1710	0.03982	1442.3	1.4423E5	3.384E-3	0.4	1.4	81.008	128.44	105.8
44.42	137.4	0.3234	22.004	22.4	708.4	1242.5300	10000	0.1739	0.03754	1553.2	1.5532E5	3.384E-3	0.4	1.4	82.004	136.29	109.9
47.17	142.8	0.3303	23.004	22.4	686.1	1343.5900	10000	0.1684	0.03365	1679.5	1.6795E5	3.384E-3	0.4	1.4	83.004	144.71	114.2
51.26	150.8	0.3399	24.004	22.4	694.4	1495.6899	10000	0.1704	0.03053	1869.6	1.8696E5	3.384E-3	0.4	1.4	84.004	157.28	120.6
54.07	155.9	0.3468	25.004	22.4	703.5	1596.9500	10000	0.1727	0.02894	1996.2	1.9962E5	3.383E-3	0.4	1.4	85.004	165.89	124.7
57.00	161.3	0.3533	26.004	22.4	690.3	1710.9800	10000	0.1694	0.02652	2138.7	2.1387E5	3.384E-3	0.4	1.4	86.004	174.86	129.1
61.17	169.3	0.3613	27.004	22.4	696.9	1882.0000	10000	0.1710	0.02431	2352.5	2.3525E5	3.383E-3	0.5	1.5	87.004	187.67	135.5
64.74	174.4	0.3711	28.004	22.4	684.5	1996.9100	10000	0.1680	0.02249	2496.1	2.4961E5	3.383E-3	0.5	1.5	88.004	198.63	139.6
67.81	179.6	0.3777	29.008	22.4	667.9	2120.6101	10000	0.1639	0.02072	2650.8	2.6508E5	3.384E-3	0.5	1.5	89.008	208.05	143.6
73.14	187.5	0.3900	30.004	22.4	670.4	2306.0200	10000	0.1645	0.01906	2882.5	2.8825E5	3.383E-3	0.5	1.5	90.004	224.40	150.0
76.09	192.7	0.3949	31.004	22.4	663.8	2432.2400	10000	0.1629	0.01788	3040.3	3.0403E5	3.383E-3	0.5	1.5	91.004	233.44	154.2
79.55	197.8	0.4021	32.004	22.4	662.1	2637.5200	10000	0.1625	0.01692	3296.9	3.2969E5	3.383E-3	0.5	1.5	92.004	244.06	158.3
84.38	205.8	0.4100	33.020	22.4	662.1	2773.6399	10000	0.1625	0.01563	3467.1	3.4671E5	3.384E-3	0.6	1.6	93.020	258.88	164.7
88.72	211.0	0.4205	34.004	22.4	646.4	2912.6399	10000	0.1587	0.01452	3640.8	3.6408E5	3.384E-3	0.6	1.6	94.004	272.20	168.8
93.17	218.6	0.4262	35.004	22.4	650.6	3128.6299	10000	0.1597	0.01361	3910.8	3.9108E5	3.384E-3	0.6	1.6	95.004	285.84	174.9
97.76	223.9	0.4366	36.004	22.4	648.1	3281.5801	10000	0.1591	0.01293	4102.0	4.1020E5	3.383E-3	0.6	1.6	96.004	299.92	179.1
101.7	229.1	0.4437	37.004	22.4	637.3	3431.7900	10000	0.1564	0.01215	4289.7	4.2897E5	3.384E-3	0.6	1.6	97.004	311.86	183.3
106.5	236.6	0.4501	38.004	22.4	618.3	3658.3101	10000	0.1518	0.01104	4572.9	4.5729E5	3.384E-3	0.6	1.6	98.004	326.73	189.3
110.0	241.8	0.4550	39.004	22.4	633.2	3822.2900	10000	0.1554	0.01083	4777.9	4.7779E5	3.384E-3	0.7	1.7	99.004	337.57	193.5
116.1	249.6	0.4651	40.004	22.4	637.3	4068.4800	10000	0.1564	0.01023	5085.6	5.0856E5	3.383E-3	0.7	1.7	100.004	356.12	199.7
120.1	254.6	0.4717	41.008	22.4	629.1	4232.6602	10000	0.1544	9.704E-3	5290.8	5.2908E5	3.384E-3	0.7	1.7	101.008	368.46	203.7
124.2	259.8	0.4779	42.004	22.4	622.5	4409.6001	10000	0.1528	9.220E-3	5512.0	5.5120E5	3.384E-3	0.7	1.7	102.004	380.98	207.9
130.3	267.6	0.4870	43.004	22.4	614.2	4675.4302	10000	0.1507	8.577E-3	5844.3	5.8443E5	3.384E-3	0.7	1.7	103.004	399.87	214.1
134.8	272.7	0.4943	44.004	22.4	610.1	4851.0698	10000	0.1497	8.206E-3	6063.8	6.0638E5	3.384E-3	0.7	1.7	104.004	413.53	218.1
139.3	280.3	0.4970	45.004	22.4	582.0	5128.8501	10000	0.1428	7.405E-3	6411.1	6.4111E5	3.383E-3	0.8	1.8	105.004	427.50	224.3
143.6	285.5	0.5029	46.004	22.4	577.8	5318.1602	10000	0.1418	7.088E-3	6647.7	6.6477E5	3.383E-3	0.8	1.8	106.004	440.53	228.4
148.7	293.1	0.5072	47.004	22.4	600.2	5601.8999	10000	0.1473	6.986E-3	7002.4	7.0024E5	3.383E-3	0.8	1.8	107.004	456.06	234.5
152.9	298.1	0.5129	48.020	22.4	579.5	5797.5698	10000	0.1422	6.519E-3	7247.0	7.2470E5	3.384E-3	0.8	1.8	108.020	469.11	238.5
156.9	303.3	0.5171	48.996	22.4	582.0	6000.6802	10000	0.1428	6.325E-3	7500.9	7.5009E5	3.384E-3	0.8	1.8	108.996	481.25	242.7
163.5	311.0	0.5258	50.004	22.4	563.8	6302.3398	10000	0.1384	5.830E-3	7877.9	7.8779E5	3.384E-3	0.8	1.8	110.004	501.63	248.8
168.9	316.0	0.5346	51.004	22.4	586.1	6510.4302	10000	0.1438	5.869E-3	8138.0	8.1380E5	3.384E-3	0.9	1.9	111.004	518.31	252.8
174.0	323.8	0.5375	52.000	22.4	558.8	6832.3301	10000	0.1372	5.330E-3	8540.4	8.5404E5	3.384E-3	0.9	1.9	112.000	533.94	259.0
183.6	328.9	0.5583	53.004	22.4	524.1	7046.5000	10000	0.1286	4.846E-3	8808.1	8.8081E5	3.384E-3	0.9	1.9	113.004	563.33	263.1
187.8	336.4	0.5582	54.004	22.4	537.3	7374.5298	10000	0.1319	4.747E-3	9218.2	9.2182E5	3.384E-3	0.9	1.9	114.004	576.12	269.1
192.4	341.6	0.5633	55.000	22.4	539.8	7603.6299	10000	0.1325	4.626E-3	9504.5	9.5045E5	3.384E-3	0.9	1.9	115.000	590.32	273.3
195.8	346.7	0.5648	56.004	22.4	536.5	7829.4199	10000	0.1317	4.463E-3	9786.8	9.7868E5	3.384E-3	0.9	1.9	116.004	600.80	277.4
202.4	354.2	0.5714	57.000	22.4	565.4	8169.0400	10000	0.1388	4.507E-3	10211	1.0211E6	3.384E-3	1.0	2.0	117.000	620.92	283.4
207.0	359.3	0.5761	58.004	22.4	544.8	8409.2500	10000	0.1337	4.219E-3	10512	1.0512E6	3.384E-3	1.0	2.0	118.004	635.11	287.5
215.7	367.0	0.5877	59.000	22.4	539.0	8775.2500	10000	0.1323	4.002E-3	10969	1.0969E6	3.383E-3	1.0	2.0	119.000	661.66	293.6
220.7	372.0	0.5933	60.004	22.4	526.6	9007.3301	10000	0.1292	3.805E-3	11259	1.1259E6	3.383E-3	1.0	2.0	120.004	677.08	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

226.9	375.0	0.6050	1.0120	22.4	485.2	200.8150	10000	0.1191	3.451E-3	251.02	25102	3.383E-3	0.0	2.0	121.012	696.03	300.0
227.0	375.0	0.6052	2.1400	22.4	497.6	577.7470	10000	0.1221	3.539E-3	722.18	72218	3.384E-3	0.0	2.0	122.140	696.30	300.0
223.9	375.0	0.5969	3.0080	22.4	480.3	829.1130	10000	0.1179	3.415E-3	1036.4	1.0364E5	3.384E-3	0.1	2.1	123.008	686.77	300.0
224.1	375.0	0.5975	4.0200	22.4	501.8	1206.1100	10000	0.1232	3.568E-3	1507.6	1.5076E5	3.384E-3	0.1	2.1	124.020	687.47	300.0
223.1	375.0	0.5949	5.0160	22.4	491.0	1457.3199	10000	0.1205	3.492E-3	1821.7	1.8217E5	3.384E-3	0.1	2.1	125.016	684.38	300.0
221.4	375.0	0.5904	6.0160	22.4	528.2	1708.8199	10000	0.1296	3.756E-3	2136.0	2.1360E5	3.384E-3	0.1	2.1	126.016	679.23	300.0
221.9	375.0	0.5918	7.0680	22.4	475.3	2085.7000	10000	0.1167	3.380E-3	2607.1	2.6071E5	3.384E-3	0.1	2.1	127.068	680.87	300.0
222.5	375.0	0.5934	8.0200	22.4	519.1	2337.1201	10000	0.1274	3.692E-3	2921.4	2.9214E5	3.383E-3	0.1	2.1	128.020	682.64	300.0
223.9	375.0	0.5970	9.0040	22.4	501.8	2714.0200	10000	0.1232	3.568E-3	3392.5	3.3925E5	3.384E-3	0.2	2.2	129.004	686.88	300.0
226.0	375.0	0.6026	10.016	22.4	496.8	2965.2100	10000	0.1219	3.533E-3	3706.5	3.7065E5	3.384E-3	0.2	2.2	130.016	693.26	300.0
221.6	375.0	0.5909	11.016	22.4	487.7	3217.9600	10000	0.1197	3.468E-3	4022.5	4.0225E5	3.384E-3	0.2	2.2	131.016	679.81	300.0
220.8	375.0	0.5887	12.020	22.4	499.3	3593.7400	10000	0.1225	3.550E-3	4492.2	4.4922E5	3.384E-3	0.2	2.2	132.020	677.32	300.0
221.7	375.0	0.5912	13.024	22.4	527.4	3846.0300	10000	0.1294	3.750E-3	4807.5	4.8075E5	3.384E-3	0.2	2.2	133.024	680.19	300.0
223.5	375.0	0.5960	14.016	22.4	524.9	4223.7700	10000	0.1288	3.733E-3	5279.7	5.2797E5	3.383E-3	0.2	2.2	134.016	685.70	300.0
222.5	375.0	0.5934	15.016	22.4	513.3	4473.3701	10000	0.1260	3.650E-3	5591.7	5.5917E5	3.384E-3	0.3	2.3	135.016	682.74	300.0
225.4	375.0	0.6011	16.016	22.4	478.6	4724.8301	10000	0.1175	3.404E-3	5906.0	5.9060E5	3.383E-3	0.3	2.3	136.016	691.55	300.0
221.2	375.0	0.5899	17.024	22.4	491.0	5101.7300	10000	0.1205	3.492E-3	6377.2	6.3772E5	3.383E-3	0.3	2.3	137.024	678.61	300.0
223.2	375.0	0.5953	18.068	22.4	503.4	5353.0000	10000	0.1236	3.580E-3	6691.3	6.6913E5	3.384E-3	0.3	2.3	138.068	684.89	300.0
222.2	375.0	0.5924	19.016	22.4	491.0	5732.8501	10000	0.1205	3.492E-3	7166.1	7.1661E5	3.384E-3	0.3	2.3	139.016	681.57	300.0
224.0	375.0	0.5973	20.016	22.4	505.9	5991.5298	10000	0.1242	3.598E-3	7489.4	7.4894E5	3.384E-3	0.3	2.3	140.016	687.12	300.0
224.3	375.0	0.5982	21.016	22.4	511.7	6233.3599	10000	0.1256	3.639E-3	7791.7	7.7917E5	3.384E-3	0.4	2.4	141.016	688.23	300.0
220.4	375.0	0.5877	22.024	22.4	495.2	6611.0801	10000	0.1215	3.521E-3	8263.9	8.2639E5	3.384E-3	0.4	2.4	142.024	676.09	300.0
221.3	375.0	0.5901	23.020	22.4	515.0	6862.2202	10000	0.1264	3.662E-3	8577.8	8.5778E5	3.384E-3	0.4	2.4	143.020	678.94	300.0
222.8	375.0	0.5941	24.020	22.4	486.9	7112.2998	10000	0.1195	3.462E-3	8890.4	8.8904E5	3.383E-3	0.4	2.4	144.020	683.58	300.0
223.1	375.0	0.5950	25.016	22.4	509.2	7489.1099	10000	0.1250	3.621E-3	9361.4	9.3614E5	3.384E-3	0.4	2.4	145.016	684.48	300.0
221.8	375.0	0.5914	26.020	22.4	508.4	7740.5801	10000	0.1248	3.615E-3	9675.7	9.6757E5	3.384E-3	0.4	2.4	146.020	680.36	300.0
221.2	375.0	0.5898	27.024	22.4	477.8	8117.5298	10000	0.1173	3.398E-3	10147	1.0147E6	3.384E-3	0.5	2.5	147.024	678.55	300.0
223.2	375.0	0.5952	28.024	22.4	539.0	8369.1504	10000	0.1323	3.833E-3	10461	1.0461E6	3.383E-3	0.5	2.5	148.024	684.78	300.0
221.8	375.0	0.5915	29.016	22.4	475.3	8620.2500	10000	0.1167	3.380E-3	10775	1.0775E6	3.383E-3	0.5	2.5	149.016	680.58	300.0
224.4	375.0	0.5983	30.016	22.4	477.8	8997.2803	10000	0.1173	3.398E-3	11247	1.1247E6	3.383E-3	0.5	2.5	150.016	688.36	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

220.7	371.8	0.5936	1.0080	22.4	511.7	235.3280	10000	0.1256	3.703E-3	294.16	29416	3.383E-3	0.0	2.5	152.008	677.00	297.4
212.7	364.3	0.5840	2.0240	22.4	509.2	592.1700	10000	0.1250	3.838E-3	740.21	74021	3.384E-3	0.0	2.6	153.024	652.68	291.4
208.5	359.2	0.5806	3.0080	22.4	558.8	830.1960	10000	0.1372	4.332E-3	1037.7	1.0377E5	3.384E-3	0.1	2.6	154.008	639.70	287.3
199.1	351.5	0.5664	4.0080	22.4	527.4	1182.7700	10000	0.1294	4.270E-3	1478.5	1.4785E5	3.384E-3	0.1	2.6	155.008	610.69	281.2
195.5	346.5	0.5643	5.0200	22.4	537.3	1420.7600	10000	0.1319	4.476E-3	1776.0	1.7760E5	3.384E-3	0.1	2.6	156.020	599.77	277.2
192.3	341.4	0.5632	6.0040	22.4	556.3	1633.9000	10000	0.1365	4.774E-3	2042.4	2.0424E5	3.384E-3	0.1	2.6	157.004	589.84	273.1
185.3	333.6	0.5554	7.0200	22.4	553.9	1972.8400	10000	0.1359	4.975E-3	2466.1	2.4661E5	3.384E-3	0.1	2.6	158.020	568.53	266.9
180.0	328.6	0.5478	8.0080	22.4	533.2	2182.6699	10000	0.1309	4.938E-3	2728.3	2.7283E5	3.384E-3	0.1	2.7	159.008	552.21	262.9
170.6	321.0	0.5314	9.0200	22.4	570.4	2502.1101	10000	0.1400	5.536E-3	3127.6	3.1276E5	3.384E-3	0.2	2.7	160.020	523.29	256.8
166.7	315.8	0.5279	10.020	22.4	576.2	2714.7100	10000	0.1414	5.777E-3	3393.4	3.3934E5	3.384E-3	0.2	2.7	161.020	511.52	252.7
162.4	308.1	0.5269	11.004	22.4	559.6	3023.3501	10000	0.1374	5.894E-3	3779.2	3.7792E5	3.384E-3	0.2	2.7	162.004	498.09	246.5
157.0	303.1	0.5181	12.004	22.4	580.3	3223.6201	10000	0.1424	6.318E-3	4029.5	4.0295E5	3.383E-3	0.2	2.7	163.004	481.73	242.5
152.3	297.9	0.5113	13.016	22.4	589.4	3421.9700	10000	0.1447	6.641E-3	4277.5	4.2775E5	3.384E-3	0.2	2.7	164.016	467.32	238.3
146.1	290.3	0.5035	14.020	22.4	583.6	3710.9199	10000	0.1432	6.927E-3	4638.7	4.6387E5	3.384E-3	0.2	2.8	165.020	448.36	232.2
141.0	285.2	0.4943	15.020	22.4	610.1	3899.2200	10000	0.1497	7.499E-3	4874.0	4.8740E5	3.383E-3	0.3	2.8	166.020	432.55	228.2
135.1	277.5	0.4868	16.012	22.4	610.1	4179.3198	10000	0.1497	7.924E-3	5224.2	5.2242E5	3.383E-3	0.3	2.8	167.012	414.41	222.0
131.3	272.3	0.4821	17.024	22.4	600.2	4360.4902	10000	0.1473	8.095E-3	5450.6	5.4506E5	3.383E-3	0.3	2.8	168.024	402.75	217.8
126.3	267.3	0.4728	18.020	22.4	620.0	4624.6001	10000	0.1522	8.681E-3	5780.8	5.7808E5	3.383E-3	0.3	2.8	169.020	387.62	213.8
121.3	259.6	0.4675	19.020	22.4	628.3	4798.4102	10000	0.1542	9.326E-3	5998.0	5.9980E5	3.384E-3	0.3	2.8	170.020	372.27	207.6
116.6	254.3	0.4586	20.020	22.4	619.2	4974.0601	10000	0.1520	9.576E-3	6217.6	6.2176E5	3.383E-3	0.3	2.9	171.020	357.74	203.4
110.9	246.6	0.4495	21.020	22.4	634.0	5218.0298	10000	0.1556	0.01042	6522.5	6.5225E5	3.384E-3	0.4	2.9	172.020	340.16	197.3
106.6	241.5	0.4415	22.020	22.4	660.5	5379.7402	10000	0.1621	0.01133	6724.7	6.7247E5	3.384E-3	0.4	2.9	173.020	327.14	193.2
104.1	236.2	0.4406	23.008	22.4	643.1	5542.3198	10000	0.1578	0.01152	6927.9	6.9279E5	3.384E-3	0.4	2.9	174.008	319.30	189.0
98.93	228.6	0.4327	24.020	22.4	631.6	5768.8101	10000	0.1550	0.01208	7211.0	7.2110E5	3.384E-3	0.4	2.9	175.020	303.52	182.9
94.82	223.5	0.4242	25.016	22.4	651.4	5917.5200	10000	0.1599	0.01304	7396.9	7.3969E5	3.383E-3	0.4	2.9	176.016	290.90	178.8
89.39	215.6	0.4146	26.032	22.4	653.9	6143.3301	10000	0.1605	0.01407	7679.2	7.6792E5	3.383E-3	0.4	3.0	177.032	274.23	172.5
86.44	210.5	0.4107	27.024	22.4	658.0	6279.8398	10000	0.1615	0.01485	7849.8	7.8498E5	3.383E-3	0.5	3.0	178.024	265.21	168.4
82.08	205.4	0.3997	28.012	22.4	663.0	6417.1699	10000	0.1627	0.01572	8021.5	8.0215E5	3.383E-3	0.5	3.0	179.012	251.83	164.3
77.12	197.4	0.3906	29.024	22.4	667.9	6623.2402	10000	0.1639	0.01713	8279.1	8.2791E5	3.383E-3	0.5	3.0	180.024	236.61	158.0
73.72	192.4	0.3832	30.024	22.4	683.6	6748.0698	10000	0.1678	0.01848	8435.1	8.4351E5	3.384E-3	0.5	3.0	181.024	226.17	153.9
70.17	184.7	0.3800	31.028	22.4	681.2	6935.4702	10000	0.1672	0.01997	8669.3	8.6693E5	3.384E-3	0.5	3.0	182.028	215.27	147.7
66.63	179.4	0.3715	32.024	22.4	674.5	7061.0400	10000	0.1656	0.02097	8826.3	8.8263E5	3.384E-3	0.5	3.1	183.024	204.42	143.5
63.19	174.0	0.3631	33.008	22.4	675.4	7179.8799	10000	0.1658	0.02230	8974.9	8.9749E5	3.383E-3	0.6	3.1	184.008	193.85	139.2
58.05	166.4	0.3489	34.016	22.4	698.5	7348.1602	10000	0.1714	0.02523	9185.2	9.1852E5	3.383E-3	0.6	3.1	185.016	178.08	133.1
55.49	161.1	0.3445	35.024	22.4	677.0	7460.6001	10000	0.1662	0.02609	9325.8	9.3258E5	3.383E-3	0.6	3.1	186.024	170.25	128.9
52.46	155.7	0.3368	36.028	22.4	698.5	7616.7002	10000	0.1714	0.02880	9520.9	9.5209E5	3.384E-3	0.6	3.1	187.028	160.95	124.6
47.91	148.1	0.3234	37.004	22.4	702.7	7716.0698	10000	0.1725	0.03203	9645.1	9.6451E5	3.384E-3	0.6	3.1	188.004	146.97	118.5
45.29	142.8	0.3171	38.028	22.4	706.8	7815.2300	10000	0.1735	0.03465	9769.0	9.7690E5	3.384E-3	0.6	3.2	189.028	138.95	114.3
42.41	137.3	0.3088	39.032	22.4	706.8	7958.8301	10000	0.1735	0.03748	9948.5	9.9485E5	3.384E-3	0.7	3.2	190.032	130.10	109.9
38.49	129.6	0.2971	40.028	22.4	721.7	8045.1802	10000	0.1771	0.04299	10056	1.0056E6	3.384E-3	0.7	3.2	191.028	118.10	103.7
36.31	124.2	0.2922	41.028	22.4	699.3	8132.8398	10000	0.1716	0.04530	10166	1.0166E6	3.384E-3	0.7	3.2	192.028	111.39	99.40
34.13	118.7	0.2875	42.028	22.4	716.7	8219.2695	10000	0.1759	0.05086	10274	1.0274E6	3.384E-3	0.7	3.2	193.028	104.71	94.97
30.08	111.0	0.2711	43.028	22.4	718.4	8332.2900	10000	0.1763	0.05835	10415	1.0415E6	3.383E-3	0.7	3.2	194.028	92.280	88.76
27.73	105.6	0.2625	44.028	22.4	729.9	8405.8203	10000	0.1792	0.06543	10507	1.0507E6	3.383E-3	0.7	3.3	195.028	85.069	84.50
24.99	100.0	0.2498	45.008	22.4	720.8	8480.1699	10000	0.1769	0.07205	10600	1.0600E6	3.383E-3	0.8	3.3	196.008	76.665	80.02
21.87	91.77	0.2383	46.008	22.4	721.7	8579.4102	10000	0.1771	0.08568	10724	1.0724E6	3.383E-3	0.8	3.3	197.008	67.099	73.42
19.83	86.39	0.2295	47.020	22.4	725.0	8641.2900	10000	0.1779	0.09713	10802	1.0802E6	3.383E-3	0.8	3.3	198.020	60.840	69.11
17.66	80.66	0.2190	48.012	22.4	730.8	8703.0498	10000	0.1794	0.1123	10879	1.0879E6	3.383E-3	0.8	3.3	199.012	54.192	64.53
16.15	74.83	0.2158	49.004	22.4	739.0	8758.8799	10000	0.1814	0.1320	10949	1.0949E6	3.383E-3	0.8	3.3	200.004	49.546	59.86
13.95	69.53	0.2006	50.008	22.4	732.4	8807.9902	10000	0.1798	0.1515	11010	1.1010E6	3.383E-3	0.8	3.4	201.008	42.792	55.63
12.11	63.81	0.1898	51.028	22.4	744.0	8882.7998	10000	0.1826	0.1827	11104	1.1104E6	3.384E-3	0.9	3.4	202.028	37.164	51.05
9.628	55.43	0.1737	52.028	22.4	748.9	8918.6797	10000	0.1838	0.2438	11148	1.1148E6	3.384E-3	0.9	3.4	203.028	29.537	44.34
8.065	50.03	0.1612	53.028	22.4	747.3	8955.4297	10000	0.1834	0.2986	11194	1.1194E6	3.384E-3	0.9	3.4	204.028	24.743	40.02
6.416	44.00	0.1458	54.008	22.4	741.5	8991.9199	10000	0.1820	0.3830	11240	1.1240E6	3.384E-3	0.9	3.4	205.008	19.683	35.20
5.019	37.70	0.1331	55.028	22.4	749.8	9022.1904	10000	0.1840	0.5275	11278	1.1278E6	3.384E-3	0.9	3.4	206.028	15.398	30.16
3.817	32.34	0.1180	56.004	22.4	748.9	9046.3701	10000	0.1838	0.7162	11308	1.1308E6	3.384E-3	0.9	3.5	207.004	11.711	25.87
2.784	25.97	0.1072	57.000	22.4	745.6	9070.1602	10000	0.1830	1.105	11338	1.1338E6	3.384E-3	1.0	3.5	208.000	8.5414	20.78
2.169	22.20	0.09769	58.016	22.4	747.3	9081.6602	10000	0.1834	1.516	11352	1.1352E6	3.384E-3	1.0	3.5	209.016	6.6531	17.76
1.077	13.76	0.07829	59.040	22.4	753.9	9098.3896	10000	0.1850	3.982	11373	1.1373E6	3.384E-3	1.0	3.5	210.040	3.3051	11.01
0.3596	6.637	0.05419	60.028	22.4	754.7	9106.2305	10000	0.1852	17.14	11383	1.1383E6	3.384E-3	1.0	3.5	211.028	1.1034	5.309

